反应详情

温度

110 °C

Next, a reaction flask was loaded with acetic acid (54 ml) and 9,10-phenanthrenequinone (3.8 g), and the temperature was raised to 110° C. with stirring to dissolve 9,10-phenanthrenequinone. To this mixture, 2-hydrazino-6-(2,2,3,3,4,4,5,5-octafluoropentyloxy)pyridine (10 g) was added in 30 minutes. After stirring at 110° C. for one hour, the reaction mixture was filtrated. Crystals were stirred in methanol (100 ml) for 30 minutes, filtrated and dried to give intended crystals (5.2 g).

1. stirringAfter stirring at 110° C. for one hour
2. filtrationthe reaction mixture was filtrated
3. stirringCrystals were stirred in methanol (100 ml) for 30 minutes
4. filtrationfiltrated
5. customdried
6. customto give