3,5-Difluorobenzaldehyde → HCID 22599530, compound

HRID 1267204Notes

Reaction equation

[F:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([F:10])[CH:9]=1)[CH:5]=[O:6].[CH3:11]CCCC.C(OCC)C>>[F:1][C:2]1[CH:3]=[C:4]([CH:5]2[O:6][CH2:11]2)[CH:7]=[C:8]([F:10])[CH:9]=1

Participants

Reactant 2

HCID 5881603,5-Difluorobenzaldehyde

HCID 21877078Diethylether pentane

Product 1

HCID 22599530HCID 22599530, compound

Procedure

Following General Procedure EC and using 3,5-difluorobenzaldehyde (Aldrich), the title compound was isolated after flash chromatography with 20:1 pentane/diethylether.

Sources & evidence

ORD record: ord-d4716c9e808c406caf5b757b5d756c89
Source dataset: uspto-grants-2003_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06552013B1

Reaction notes

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