HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23500527, compound → HCID 23500548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23500527 | HCID 23500527 | — |
| Reactant | Sodium periodate | HCID 23667635 | — |
| Catalyst | Osmium Tetroxide | HCID 30318 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 23500548 | HCID 23500548 | — |
Reaction Steps
To a solution of the product of Example 18 in dioxane and water is added sodium periodate and osmium tetraoxide. The reaction is stirred at room temperature and monitored by thin layer chromatography. Water is added to the reaction mixture and the solution is extracted with CH2Cl2. The organic layer is dried over magnesium sulfate, filtered, and stripped of all solvent under reduced pressure to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06552052B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-871b15e5158243d59e2847b1daa72b34 |
| Source note | uspto-grants-2003_04 |