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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1267318생성일: 2026년 10월 26일

(Z)-2-[3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]-2-propenyl]-1,3-dioxane → 2-[3-[4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propyl]-1,3-dioxane

https://huagongshe.com/reaction/1267318

반응식

참여 물질

역할이름HCID투입량
반응물(Z)-2-[3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]-2-propenyl]-1,3-dioxaneHCID 11811571—
촉매HCID 178418390HCID 178418390—
용매EthanolHCID 702—
생성물2-[3-[4-[2-(5-Methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propyl]-1,3-dioxaneHCID 1102590296%

반응 단계

A mixture of (Z)-2-[3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]-2-propenyl]-1,3-dioxane (5.0 g), palladium-carbon (5%, 0.1 g) and ethanol (100 ml) was subjected to catalytic hydrogenation at room temperature under one atmospheric pressure. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure. The concentrate was purified by means of a silica gel column chromatography. From the fractions eluted with hexane-ethyl acetate (1:1), 2-[3-[4-[2-(5-methyl-2-phenyl-4-oxazolyl)ethoxy]phenyl]propyl]-1,3-dioxane (4.8 g, 96%) was obtained.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06552058B1
출처 데이터셋uspto-grants-2003_04
ORD IDord-97e3880186d142199c0524b6392b3c3c
출처 메모uspto-grants-2003_04