HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 18545696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 18545677 | HCID 18545677 | — |
| Product | HCID 18545696 | HCID 18545696 | 100.2% |
Reaction Steps
A mixture of 6 g (0.014 mole) of 4-[(8-phenethyl-8-azabicyclo[3.2.1]oct-3-ylidene)phenylmethyl]benzoic acid, 20 ml of CHCl2 and 3 mL (0.042 mole) of thionyl chloride were refluxed for 1.5 h. The solvent was evaporated in vacuo to give 6.2 g of 4-[(8-phenethyl-8-azabicyclo[3.2.1]oct-3-ylidene)phenylmethyl]benzoyl chloride. MS m/z (MH+) of CH3OH quench 437.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06552036B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-c844fe8444bd4521a7b657272a4f7ce5 |
| Source note | uspto-grants-2003_04 |