Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Isobutylene | HCID 8255 | — |
| Reactant | HCID 21930687 | HCID 21930687 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22650062 | HCID 22650062 | 81% |
Reaction Steps
A mixture of 5 mmole of the above-prepared 1-acryloyloxy-3-carboxyadamantane, 50 mmole of isobutene, 0.5 mmole of sulfuric acid and 50 ml of dichloromethane was stirred at 0° C. for 24 hours. After concentrating the reaction mixture, the concentrate was subjected to column chromatography on a silica gel to thereby yield the title compound in a yield of 81%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06552143B2 |
|---|
| Source dataset | uspto-grants-2003_04 |
|---|
| ORD ID | ord-a6d05be4165e4d6581c69e6668b53ba5 |
|---|
| Source note | uspto-grants-2003_04 |
|---|
