Acryloyl chloride → HCID 22650072, compound

HRID 1267553Notes

Reaction equation

HRID 1267553 reaction equation
[O:1]1[CH:7]2[CH:2]1[C:3]([O:5][C:6]2([CH3:9])[CH3:8])=[O:4].[C:10](Cl)(=[O:13])[CH:11]=[CH2:12]>>[C:10]([O:1][CH:7]1[C:6]([CH3:8])([CH3:9])[O:5][C:3](=[O:4])[CH2:2]1)(=[O:13])[CH:11]=[CH2:12]

Participants

3

Reactant 2

HCID 13140Acryloyl chlorideHCID 22650065HCID 22650065, compound

Product 1

HCID 22650072HCID 22650072, compoundYield 87%

Procedure

The above-prepared 3-hydroxy-4,4-dimethyl-γ-butyrolactone was allowed to react with acryloyl chloride in a similar manner to that in Production Example 22 to thereby yield the title compound in a yield of 87%.

Sources & evidence

ORD record
ord-4d74f9a55b9b4802951df2eef1fe6cae
Source dataset
uspto-grants-2003_04
Patent number
US06552143B2

Reaction notes

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