Acryloyl chloride → HCID 22650073, compound

HRID 1267554Notes

Reaction equation

HRID 1267554 reaction equation
[O:1]1[C:7]2([CH3:8])[CH:2]1[C:3]([O:5][C:6]2([CH3:10])[CH3:9])=[O:4].[C:11](Cl)(=[O:14])[CH:12]=[CH2:13]>>[C:11]([O:1][C:7]1([CH3:8])[C:6]([CH3:9])([CH3:10])[O:5][C:3](=[O:4])[CH2:2]1)(=[O:14])[CH:12]=[CH2:13]

Participants

3

Reactant 2

HCID 13140Acryloyl chlorideHCID 22650068HCID 22650068, compound

Product 1

HCID 22650073HCID 22650073, compoundYield 85%

Procedure

The above-prepared 3-hydroxy-3,4,4-trimethyl-γ-butyrolactone was allowed to react with acryloyl chloride in a similar manner to that in Production Example 22 to thereby yield the title compound in a yield of 85%.

Sources & evidence

ORD record
ord-efd8efbf423c4ee2987a50cef823363c
Source dataset
uspto-grants-2003_04
Patent number
US06552143B2

Reaction notes

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