3,4-Dimethoxyphenylboronic acid → HCID 18546796, compound

HRID 1267636Notes

Reaction equation

HRID 1267636 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5](B(O)O)[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].Cl[C:15]1[CH:16]=[C:17]([CH:23]=[CH:24][N:25]=1)[C:18]([O:20][CH2:21][CH3:22])=[O:19]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:15]2[CH:16]=[C:17]([CH:23]=[CH:24][N:25]=2)[C:18]([O:20][CH2:21][CH3:22])=[O:19])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10]

Participants

3

Reactant 2

HCID 27347023,4-Dimethoxyphenylboronic acidHCID 2762942Ethyl 2-chloroisonicotinate

Product 1

HCID 18546796HCID 18546796, compound

Procedure

3,4-Dimethoxyphenylboronic acid (215 mg) and ethyl 2-chioroisonicotinate (200 mg) were treated in the same manner as in Preparation Example 1 to obtain the title compound.

Sources & evidence

ORD record
ord-7d3610df3d9649c3afd531b540d95d53
Source dataset
uspto-grants-2003_04
Patent number
US06552188B2

Reaction notes

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