HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1267683Generated: October 31, 2026
O-Xylene → Methyl 1-methylcyclopropane-1-carboxylate
https://huagongshe.com/reaction/1267683
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | Methyl 4-Chloro-2-methylbutyrate | HCID 11263584 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 1-methylcyclopropane-1-carboxylate | HCID 543995 | — |
| Product | Methyl 4-Chloro-2-methylbutyrate | HCID 11263584 | — |
Reaction Steps
contacting the xylene solution of methyl 4-chloro-2-methylbutyrate from step (3) with an sodium methoxide and heating at temperatures of about 100 to 200° C. which causes vaporization of (i) methanol as it is formed and (ii) methyl 1-methylcyclopropanecarboxylate as it is formed from methyl 4-chloro-2-methylbutyrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06552217B2 |
|---|
| Source dataset | uspto-grants-2003_04 |
|---|
| ORD ID | ord-06594cb39e2b46899741b890488f1755 |
|---|
| Source note | uspto-grants-2003_04 |
|---|
