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HRID 1267759作成日：2026年10月25日

10-[(3RS,4RS)-3-ethyl-7-hydroxy-3-(4-hydroxyphenyl)thiochroman-4-yl]-2-(7,7,8,8,8-pentafluoro-octyl)decanoic acid → 10-[(3RS,4RS)-3-ethyl-7-hydroxy-3-(4-hydroxyphenyl)thiochroman-4-yl]-2-(6,6,7,7,7-pentafluoroheptyl)decanoic acid

https://huagongshe.com/reaction/1267759

反応式

関与物質

役割名称HCID仕込み量
反応物10-[(3RS,4RS)-3-ethyl-7-hydroxy-3-(4-hydroxyphenyl)thiochroman-4-yl]-2-(7,7,8,8,8-pentafluoro-octyl)decanoic acidHCID 18546277—
反応物Ethyl 2-(6,6,7,7,7-pentafluoroheptyl)-8-nonenoateHCID 22718078—
生成物10-[(3RS,4RS)-3-ethyl-7-hydroxy-3-(4-hydroxyphenyl)thiochroman-4-yl]-2-(6,6,7,7,7-pentafluoroheptyl)decanoic acidHCID 10189677—

反応手順

Starting with the allyl compound prepared in Example 13 and the ethyl 2-(6,6,7,7,7-pentafluoroheptyl)-8-nonenoate prepared in Example 11, the same procedure as shown in Example 13 was repeated to give 10-[(3RS,4RS)-3-ethyl-7-hydroxy-3-(4-hydroxyphenyl)thiochroman-4-yl]-2-(6,6,7,7,7-pentafluoroheptyl)decanoic acid.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06552068B1
出典データセットuspto-grants-2003_04
ORD IDord-8b20026a970944769d89f48a67092507
出典メモuspto-grants-2003_04