2-Phenylethanol → HCID 69830311, compound

Participants

Reaction Steps

To a solution of 3,4-epoxy-3,4-dihydro-2,2-dimethyl-6-(4-methoxyphenylacetylamino)-2H-1-benzopyran (200 mg, 0.68 mmol) and phenethyl alcohol (0.32 mL, 2.72 mmol) in acetonitrile (1.0 mL), sulfuric acid (0.01 mL) was added and stirred at the room temperature for 2 hours. Thereto, ice-cooled ethyl acetate was added and the formed crystals were filtered, to obtain the intended substance as white solid (yield:77%).

Provenance & Evidence