HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminum hydride → HCID 69796253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminum hydride | HCID 14487 | — |
| Reactant | HCID 22718800 | HCID 22718800 | — |
| Product | HCID 69796253 | HCID 69796253 | — |
Reaction Steps
(E)-3-(4′-bromo-biphenyl-4-yl)-but-2-en-1-ol was prepared from (E)-3-(4′-bromo-biphenyl-4-yl)-but-2-enoic acid ethyl ester (3.45 g, 10.0 mmol) and DIBAL-H (1M in toluene, 40 ml, 40 mmol) by a procedure analogous to that described in example 1b, yielding 1.68 g (55%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06555577B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-155140a8b9784406b23206d0a2731838 |
| Source note | uspto-grants-2003_04 |