HCID 10765851, compound → 5,5-Dimethyl-10-hydroxy-8-(3-methyl-2-octyl)-5H-[1]benzopyrano[3,4-d]pyridine

Participants

Reaction Steps

A mixture of 2.23 g. of 2-benzyl-5,5-dimethyl-10-hydroxy-8-(3-methyl-2-octyl)-1,2,3,4-tetrahydro-5H-[1]benzopyrano[3,4-d]pyridine, 0.8 g. (10%) palladium on carbon, and 100 ml. of xylene was stirred and refluxed for 24 hours. After removal of the catalyst, the filtrate was evaporated in vacuo and the residue was recrystallized from acetonitrile; m.p. 154°-156°.

Provenance & Evidence