HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Phenylphenyl)boronic acid → (E)-Ethyl 3-[1,1';3',1'']terphenyl-4''-yl-but-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Phenylphenyl)boronic acid | HCID 2734315 | — |
| Reactant | (E)-ethyl 3-(4-bromophenyl)-but-2-enoate | HCID 15933615 | — |
| Product | (E)-Ethyl 3-[1,1';3',1'']terphenyl-4''-yl-but-2-enoate | HCID 22557623 | 68% |
Reaction Steps
(E)-Ethyl 3-[1,1′;3′,1″]terphenyl-4″-yl-but-2-enoate (1.02 g, 68% yield) was prepared from 3-biphenylboronic acid (1.31 g, 6.60 mmol) and (E)-ethyl 3-(4-bromophenyl)-but-2-enoate (1.0 g, 4.40 mmol) by a procedure analogous to that described in example 52a.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06555577B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-d30a314f8f9b4d73a3f2476312002045 |
| Source note | uspto-grants-2003_04 |