HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl (2S)-2-ethoxy-3-(4-hydroxyphenyl)propanoate → (E)-(S)-Ethyl 2-Ethoxy-3-[4-(3-[1,1';3',1'']terphenyl-4''-yl-but-2-enyloxy)-phenyl]-propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl (2S)-2-ethoxy-3-(4-hydroxyphenyl)propanoate | HCID 9816147 | — |
| Reactant | (E)-3-[1,1';3',1'']terphenyl-4''-yl-but-2-en-1-ol | HCID 20765800 | — |
| Product | (E)-(S)-Ethyl 2-Ethoxy-3-[4-(3-[1,1';3',1'']terphenyl-4''-yl-but-2-enyloxy)-phenyl]-propionate | HCID 20765808 | 80% |
Reaction Steps
The title compound (0.41 g, 80% yield) was prepared from (E)-3-[1,1′;3′,1″]terphenyl-4″-yl-but-2-en-1-ol (0.30 g, 1.0 mmol) and (S)-ethyl 2-ethoxy-3-(4-hydroxyphenyl)-propionate (0.25 g, 1.05 mmol) by a procedure analogous to that described in example 52c.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06555577B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-4d5b65c86c6645749f65d224fc9fcb58 |
| Source note | uspto-grants-2003_04 |