HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminum hydride → (E)-3-(4-iodophenyl)-but-2-en-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminum hydride | HCID 14487 | — |
| Reactant | (E)-ethyl 3-(4-iodophenyl)-but-2-enoate | HCID 11438459 | — |
| Product | (E)-3-(4-iodophenyl)-but-2-en-1-ol | HCID 11437263 | — |
Reaction Steps
(E)-3-(4-Iodophenyl)-but-2-en-1-ol was prepared by DIBAL-H reduction of (E)-ethyl 3-(4-iodophenyl)-but-2-enoate (example 91a) by a procedure analogous to that described in example 50b.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06555577B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-849e4768ca8f447db4834d91fee6349d |
| Source note | uspto-grants-2003_04 |