HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dichlorophenylboronic acid → (E)-ethyl 3-(3',5'-dichloro-biphenyl-4-yl)-but-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dichlorophenylboronic acid | HCID 2734331 | — |
| Reactant | (E)-ethyl 3-(4-iodophenyl)-but-2-enoate | HCID 11438459 | — |
| Product | (E)-ethyl 3-(3',5'-dichloro-biphenyl-4-yl)-but-2-enoate | HCID 22557629 | — |
Reaction Steps
The colourless solid (E)-ethyl 3-(3′,5′-dichloro-biphenyl-4-yl)-but-2-enoate was prepared from (E)-ethyl 3-(4-iodophenyl)-but-2-enoate (example 91a) and 3,5-dichlorobenzene boronic acid by a procedure analogous to that described in example 52a.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06555577B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-27948af550064940a7a14b4ce040b82a |
| Source note | uspto-grants-2003_04 |