1-[1-(Methoxyimino)-2,3-dihydro-1H-inden-5-yl]-2-(pyridin-4-yl)ethane-1,2-dione → HCID 86760478, compound

HRID 1268909Notes

Reaction equation

HRID 1268909 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][N:5]1[CH2:10][CH2:9][CH:8]([C:11]2[NH:12][C:13]([C:27]3[CH:32]=[CH:31][N:30]=[CH:29][CH:28]=3)=[C:14]([C:16]3[CH:17]=[C:18]4[C:22](=[CH:23][CH:24]=3)[C:21](=[N:25][OH:26])[CH2:20][CH2:19]4)[N:15]=2)[CH2:7][CH2:6]1.[CH3:33]ON=C1C2C(=CC(C(=O)C(C3C=CN=CC=3)=O)=CC=2)CC1>>[CH3:33][O:26][N:25]=[C:21]1[C:22]2[C:18](=[CH:17][C:16]([C:14]3[N:15]=[C:11]([CH:8]4[CH2:7][CH2:6][N:5]([CH2:4][CH2:3][O:2][CH3:1])[CH2:10][CH2:9]4)[NH:12][C:13]=3[C:27]3[CH:28]=[CH:29][N:30]=[CH:31][CH:32]=3)=[CH:24][CH:23]=2)[CH2:19][CH2:20]1

Participants

3

Reactant 2

HCID 534201501-[1-(Methoxyimino)-2,3-dihydro-1H-inden-5-yl]-2-(pyridin-4-yl)ethane-1,2-dioneHCID 136411696HCID 136411696, compound

Product 1

HCID 86760478HCID 86760478, compoundYield 32%

Procedure

The title compound (0.27 g, 32%) was prepared from the product of Step 1 and the product of Example 1 Step 4 as described in Example 1 Step 5; MS(AP+) m/e 446 [M+H]+.

Sources & evidence

ORD record
ord-060921e64562495cbbc14c6b892ac5b7
Source dataset
uspto-grants-2007_04
Patent number
US07199137B2

Reaction notes

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