HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Tert-butylphenoxy)acetic acid → HCID 69504518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Tert-butylphenoxy)acetic acid | HCID 15718 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | (S)-4-Benzyl-2-oxazolidinone | HCID 736225 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 69504518 | HCID 69504518 | — |
Reaction Steps
The target compound (28.3 g) was obtained as colorless crystals by carrying out the reaction and the post-treatment according to Reference example 20(a) using 4-t-butylphenoxyacetic acid (17.0 g), oxalyl chloride (17.8 ml), (S)-4-benzyl-2-oxazolidinone (14.2 g) and a solution of n-butyl lithium in hexane (1.61N, 50.4 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07199139B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-56e271750d2646f19d9aff97610c3722 |
| Source note | uspto-grants-2007_04 |