HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 69504410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-Fluorophenoxyacetic acid | HCID 67882 | — |
| Reactant | (S)-4-Benzyl-2-oxazolidinone | HCID 736225 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 69504410 | HCID 69504410 | — |
Reaction Steps
The target compound (2.76 g) was obtained as colorless crystals by carrying out the reaction and the post-treatment according to Reference example 20(a) using 4-fluorophenoxyacetic acid (1.70 g), oxalyl chloride (2.18 ml), (S)-4-benzyl-2-oxazolidinone (1.77 g) and a solution of n-butyl lithium in hexane (1.61N, 7.14 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07199139B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-b417122bf88a4ea98bcb25b231576075 |
| Source note | uspto-grants-2007_04 |