HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 70564567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 70564014 | HCID 70564014 | — |
| Product | HCID 70564567 | HCID 70564567 | — |
Reaction Steps
This compound was prepared in a manner analagous to Example 2, using 8.1 g of trans-4-amino-1-cyclohexyl-3-pyrrolidinol, 10 g of potassium carbonate and 6.2 g of benzoyl chloride. After filtration and solvent evaporation, the residue crystallized and was recrystallized from acetone. Yield was 5.8 g (45%), m.p. 154.0°-155.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04254135 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-51bd47b485004a41b2381dce0e0df48c |
| Source note | uspto-grants-1981_03 |