Isoprene → Isoprene butadiene
Reaction equation
[CH2:1]=[CH:2][C:3](=[CH2:5])[CH3:4].[CH2:6]=[CH:7][CH:8]=[CH2:9]>>[CH2:1]=[CH:2][C:3](=[CH2:4])[CH3:5].[CH2:6]=[CH:7][CH:8]=[CH2:9]Participants
3
Reactant 2
Product 1
Procedure
In this experiment, a 30/70 isoprene-butadiene rubber (IBR) was prepared using a preformed catalyst described in Example 2. The procedure described in Example 3 was utilized in this examples except that a premix containing a 30:70 mixture of isoprene and 1,3-butadiene was used as the monomers. GC analysis of the residual monomer indicated that 90 percent of monomers were consumed after 9 minutes. The polymerization was continued for an additional 21 minutes.
Workup
- additioncontaining
- customwere consumed after 9 minutes
Sources & evidence
- ORD record
- ord-2c4143c796a04f889094fbf8a933ca2c
- Source dataset
- uspto-grants-2007_04
- Patent number
- US07199201B2
Reaction notes
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