HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-nitrophenol → HCID 18446858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-nitrophenol | HCID 24364 | — |
| Reactant | Isobutyryl chloride | HCID 62325 | — |
| Reactant | Tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,2,3,6-tetrahydropyridine-1-carboxylate | HCID 4642098 | — |
| Reactant | HCID 18446875 | HCID 18446875 | — |
| Product | HCID 18446858 | HCID 18446858 | — |
Reaction Steps
Prepared by the procedure for N-[4-methoxy-3-(4-piperidinyl)phenyl]-2-methylpropanamide using tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3,6-dihydro-1(2H)-pyridinecarboxylate and 4-bromo-2-nitrophenol and acylating with isobutyryl chloride: ESMS m/e: 263.4 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07199135B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-967de534a3fd4c41b408f9cd15fc88df |
| Source note | uspto-grants-2007_04 |