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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1269356Generated: October 31, 2026

Trifluoroacetic acid → HCID 10257299, compound

https://huagongshe.com/reaction/1269356

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 10461521HCID 10461521—
ProductHCID 10257299HCID 10257299—

Reaction Steps

The titled compound (0.25 g) was obtained as a white powder after a TFA treatment of the (1S)-2-tert-butoxy-1-methyl-2-oxoethyl (2Z)-3-[4-(methylsulfonyl)phenyl]-4-{[6-(nitrooxy)hexanoyl]oxy}-2-phenylbut-2-enoate as prepared above. 1H NMR (500 MHz, Acetone-d6): δ 7.80 (d, 2 H), 7.48 (d, 2 H), 7.17–7.09 (m, 5 H), 5.34 (s, 2 H), 5.25 (m, 1 H), 4.50 (t, 2 H), 3.08 (s, 3 H), 2.25 (t, 2 H), 1.69 (m, 2 H), 1.55 (d, 3 H), 1.49 (m, 2 H), 1.32 (m, 2 H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07199154B2
Source datasetuspto-grants-2007_04
ORD IDord-ce22db8c2e244202ba83314fb11acbcb
Source noteuspto-grants-2007_04