Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Chlorophenol → 4-Chlorophenyl 4-(hexadecylamino)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Chlorophenol | HCID 4684 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 4-Hexadecylaminobenzoyl chloride hydrochloride | HCID 13255322 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-Chlorophenyl 4-(hexadecylamino)benzoate | HCID 23457777 | — |
반응 단계
To a solution of 6.4 g. (50 m moles) 4-chlorophenol and 7.6 g. (75 m moles) triethylamine in 500 ml. methylene chloride is added 10.4 g. (25 m moles) 4-(hexadecylamino)benzoyl chloride hydrochloride in 250 ml. methylene chloride. After four hours at reflux, the solution is cooled, washed with water and dilute phosphoric acid, and dried. After passing the solution through a column of alumina, the solvent is evaporated and the residue is crystallized from diisopropyl ether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04254138 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-f0190ceb69e644dda50395a5f4a31a74 |
| 출처 메모 | uspto-grants-1981_03 |