HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Oxide → 2-(4-Vinylphenoxy)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Oxide | HCID 6354 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Ethenylphenyl acetate | HCID 75821 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(4-Vinylphenoxy)ethanol | HCID 14937811 | — |
Reaction Steps
Para-(hydroxyethoxy)styrene was prepared using the method described in Example 1, except that the following amounts of reagents were used: 86 g (0.53 mol, 1 eq) of p-acetoxystyrene, 3.7 g (26.77 mmol, 0.05 eq) of anhydrous potassium carbonate, and 35 g (0.795 mol, 1.5 eq) of ethylene oxide in 530 mL of methanol. The isolated product yield was 61.9%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07199272B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-9e5cccfd1af64759a38e6719ece0abb4 |
| Source note | uspto-grants-2007_04 |