2-Methoxyethylamine → Ethyl (4-{[(2-methoxyethyl)amino]methyl}-2-methylphenoxy)acetate

Participants

Reaction Steps

Prepared using 2-methoxyethylamine (1.4 mL, 16.2 mmol) and the synthetic procedure described for Intermediate 7. Purification of the crude product by SCX SPE (5×10 g) loading and washing with EtOH and then eluting product with 5% NH3 in EtOH, and removal of the solvent in vacuo yielded the title compound as a brown oil (1.8 g).

Provenance & Evidence