HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 20571388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Benzeneacetic acid, 4-chloro-alpha-(1-methylethyl)- | HCID 16197 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Product | HCID 20571388 | HCID 20571388 | — |
Reaction Steps
Following the methods of Example 1, 2-(4-chlorophenyl)-3-methylbutanoic acid is reacted with oxalyl chloride and aqueous methylamine to give N-methyl-2-(4-chlorophenyl)-3-methylbutyramide, which is then combined with 3-phenoxybenzyl bromide and AgBF4, yielding 3-phenoxybenzyl N-methyl-2-(4-chlorophenyl)-3-methylbutanimidate, MS m/e 407 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04254264 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-f22e67409f3745d498d28c7d45897e05 |
| Source note | uspto-grants-1981_03 |