HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetyl chloride → 4-(2,3-Dimethoxy-benzylidene)-morpholin-4-ium chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetyl chloride | HCID 6367 | — |
| Edukt | Morpholine | HCID 8083 | — |
| Edukt | 2,3-Dimethoxybenzaldehyde | HCID 66581 | — |
| Produkt | 4-(2,3-Dimethoxy-benzylidene)-morpholin-4-ium chloride | HCID 22174759 | — |
Reaktionsschritte
The reaction of 7.3 ml (0.084 mol) morpholine and 5.8 g (0.035 mol) 2,3-dimethoxybenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 2.1 ml (0.035 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.6 g (corresponding to 59% of the yield calculated by theory) 4-(2,3-dimethoxy-benzylidene)-morpholin-4-ium chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07202242B2 |
| Quelldatensatz | uspto-grants-2007_04 |
| ORD ID | ord-cf0a4b5522694b0aa1b8037a844126f6 |
| Quellennotiz | uspto-grants-2007_04 |