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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1270111Erstellt: 25. Oktober 2026

Acetyl chloride → 4-(2,3-Dimethoxy-benzylidene)-morpholin-4-ium chloride

https://huagongshe.com/reaction/1270111

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetyl chlorideHCID 6367—
EduktMorpholineHCID 8083—
Edukt2,3-DimethoxybenzaldehydeHCID 66581—
Produkt4-(2,3-Dimethoxy-benzylidene)-morpholin-4-ium chlorideHCID 22174759—

Reaktionsschritte

The reaction of 7.3 ml (0.084 mol) morpholine and 5.8 g (0.035 mol) 2,3-dimethoxybenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 2.1 ml (0.035 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.6 g (corresponding to 59% of the yield calculated by theory) 4-(2,3-dimethoxy-benzylidene)-morpholin-4-ium chloride.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07202242B2
Quelldatensatzuspto-grants-2007_04
ORD IDord-cf0a4b5522694b0aa1b8037a844126f6
Quellennotizuspto-grants-2007_04