Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | HCID 68676574 | HCID 68676574 | — |
| Product | HCID 86594419 | HCID 86594419 | — |
Reaction Steps
The product from Step A was dissolved in 10 equiv. of ethylenediamine and heated at 138° C. in a sealed tube for 18 hrs. The excess ethylenediamine was removed by distillation to provide the title compound as a brown oil. MS (M+H)+=207.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07202245B2 |
|---|
| Source dataset | uspto-grants-2007_04 |
|---|
| ORD ID | ord-d59d6e4278dc4778a47b9edc6d8370bc |
|---|
| Source note | uspto-grants-2007_04 |
|---|
