反应详情

Morpholine (1.2 g, 14.12 mmol) was added to a stirring solution of 3,4,5-trifluoronitro benzene (1 g, 5.65 mmol) in acetonitrile (15 mL) and the reaction mixture was refluxed for 5 h. A viscous liquid was obtained upon concentration, which was then poured into crushed ice. The solid thus obtained was filtered off and dried under reduced pressure to obtain the title compound (1.2 g, 88%).

1. temperaturethe reaction mixture was refluxed for 5 h
2. customA viscous liquid was obtained upon concentration, which
3. additionwas then poured
4. custominto crushed ice
5. customThe solid thus obtained
6. filtrationwas filtered off
7. customdried under reduced pressure