HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Methoxyphenyl)-1,1-dimethylethylamine → HCID 22640855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Methoxyphenyl)-1,1-dimethylethylamine | HCID 91892 | — |
| Reactant | 2-Chloro-6-[(oxiran-2-yl)methoxy]benzonitrile | HCID 22640840 | — |
| Product | HCID 22640855 | HCID 22640855 | 143.2% |
Reaction Steps
Using the method of Example 6, supra, 3-chloro-2-cyanophenyl glycidyl ether (0.093 g, 0.44 mmol) and 1,1-dimethyl-(4-methoxyphenyl)ethylamine (0.095 g, 0.53 mmol) were used to prepare 134 mg of the title compound as a white solid: 1H-NMR (CDCl3) ∂ 9.68 (1H, br s), 8.2 (1H, br s), 7.4 (1H, t), 7.15 (2H, d), 7.03 (1H, d), 6.95 (1H, d), 6.8 (2H, d), 5.7 (1H, br s), 4.8 (1H, m), 4.3 (2H, d), 3.75 (3H, s), 3.4 (2H, m), 3.13 (2H, dd), 1.44 (3H, s), 1.40 (3H, s)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202261B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-4ea0a70751f74fad98a3e229f4f268c5 |
| Source note | uspto-grants-2007_04 |