HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl glycidyl ether → HCID 22640907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl glycidyl ether | HCID 31217 | — |
| Reactant | HCID 53761145 | HCID 53761145 | — |
| Product | HCID 22640907 | HCID 22640907 | — |
Reaction Steps
Using the method of Example 6, supra, phenyl glycidyl ether (150 mg, 1.1 mmol) and 1,1-dimethyl-2-(3-fluoro-4-methoxyphenyl)ethylamine (197 mg, 1 mmol) were used to prepare the title compound. The title compound crystallized on standing to yield 169 mg of small crystals: GC/EI-MS, m/z (rel. int.) 332 (M+−15, 0.1), 209 (16), 208 (100), 139 (13), 133 (5), 114 (7), 107 (6), 77 (11), 71 (12), 70 (20), 58 (9).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07202261B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-2dc0b205c0e14f7c8b44f485b48eff74 |
| Source note | uspto-grants-2007_04 |