HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylene → 1-Chloro-1-octen-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylene | HCID 6326 | — |
| Reactant | Hexanoyl chloride | HCID 67340 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | 1-Chloro-1-octen-3-one | HCID 54514915 | 94% |
Reaction Steps
This compound is prepared according to the procedure of Price and Pappalardo [C. C. Price and J. A. Pappalardo, Org. Syn, 32, 27 (1952)] from hexanoyl chloride, acetylene, and aluminum chloride in 94% yield, bp 51°-52° C. (0.1 mm); λ max 1680, 1595, 941 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04254285 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-c71981136930439f9fc57a6a9cfed018 |
| Source note | uspto-grants-1981_03 |