3,5-Dimethylphenol → HCID 11229923, compound

HRID 1270704Notes

Reaction equation

HRID 1270704 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[C:6]([CH3:8])[CH:7]=1.IC1C=CC=CC=1.I[C:18]1[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][CH:19]=1>>[CH3:25][O:24][C:21]1[CH:22]=[CH:23][C:18]([O:9][C:4]2[CH:5]=[C:6]([CH3:8])[CH:7]=[C:2]([CH3:1])[CH:3]=2)=[CH:19][CH:20]=1

Participants

4

Reactant 3

HCID 79483,5-Dimethylphenol2×HCID 11575IodobenzeneHCID 696764-Iodoanisole

Product 1

HCID 11229923HCID 11229923, compound

Procedure

Example 3.1 was repeated, replacing the phenol with 244 mg of 3,5-dimethylphenol (2 mmoles) and the iodobenzene with 655 mg of 4-iodoanisole (2.8 mmoles), the latter being added at the same time as the 3,5-dimethylphenol, and taking the reaction time to 48 hours.

Workup

  1. customto 48 hours

Sources & evidence

ORD record
ord-0cc5f013871d45358249e83efd159cff
Source dataset
uspto-grants-2007_04
Patent number
US07202367B2

Reaction notes

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