HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 21873584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 2-Fluoro-4-hydroxybenzonitrile | HCID 2734675 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21873584 | HCID 21873584 | — |
Reaction Steps
This was prepared by from 2-fluoro-4-hydroxy-benzonitrile by nitration (concentrated nitric acid in acetic acid at 40° C.) followed by hydrogenation in ethanol over 10% palladium/carbon.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07205408B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-bccfb429fbf64628b176e1b3f3dbb74b |
| Source note | uspto-grants-2007_04 |