HCID 10362721, compound → HCID 10088749, compound

HRID 1271857Notes

Reaction equation

HRID 1271857 reaction equation
C(OC(=O)[NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[S:21][C:20]2[CH:22]=[CH:23][C:24]([O:26][CH2:27][CH2:28][O:29][CH3:30])=[CH:25][C:19]=2[CH:18]=1)=[O:16])(C)(C)C.NC1C=CC=CC=1NC(C1SC2C=CC(OCCOCCOC)=CC=2C=1)=O>>[NH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[S:21][C:20]2[CH:22]=[CH:23][C:24]([O:26][CH2:27][CH2:28][O:29][CH3:30])=[CH:25][C:19]=2[CH:18]=1)=[O:16]

Participants

3

Reactant 2

HCID 10362721HCID 10362721, compoundHCID 69487315HCID 69487315, compound

Product 1

HCID 10088749HCID 10088749, compound

Procedure

was prepared from (2-{[5-(2-Methoxy-ethoxy)-benzo[b]thiophene-2-carbonyl]-amino}-phenyl)-carbamic acid tert-butyl ester (30) in an analogous manner to that described for the preparation of (27) example 11, step 2; yellow solid, mp. 162–165° C.

Sources & evidence

ORD record
ord-63b1614887b3481b891adc9a1b1db396
Source dataset
uspto-grants-2007_04
Patent number
US07208491B2

Reaction notes

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