HCID 10362721, compound → HCID 11726625, compound
Reaction equation
C(OC(=O)[NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[O:18][C:19]2[C:25]([O:26][CH2:27][CH2:28][O:29][CH2:30][CH2:31][O:32][CH3:33])=[CH:24][CH:23]=[CH:22][C:20]=2[CH:21]=1)=[O:16])(C)(C)C.NC1C=CC=CC=1NC(C1SC2C=CC(OCCOCCOC)=CC=2C=1)=O>>[NH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[O:18][C:19]2[C:25]([O:26][CH2:27][CH2:28][O:29][CH2:30][CH2:31][O:32][CH3:33])=[CH:24][CH:23]=[CH:22][C:20]=2[CH:21]=1)=[O:16]Participants
3
Procedure
was prepared from [2-({7-[2-(2-Methoxy-ethoxy)-ethoxy]-benzofuran-2-carbonyl}-amino)-phenyl]-carbamic acid tert-butyl ester (32) in an analogous manner to that described for the preparation of (27) example 11, step 2; exact MW [M+H] calc'd: 371.16; MW found [M+H]: 371.2.
Sources & evidence
- ORD record
- ord-2d9d25fe53e644ec90b40191b28b21f2
- Source dataset
- uspto-grants-2007_04
- Patent number
- US07208491B2
Reaction notes
Loading…