HCID 10362721, compound → HCID 11726625, compound

HRID 1271858Notes

Reaction equation

HRID 1271858 reaction equation
C(OC(=O)[NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[O:18][C:19]2[C:25]([O:26][CH2:27][CH2:28][O:29][CH2:30][CH2:31][O:32][CH3:33])=[CH:24][CH:23]=[CH:22][C:20]=2[CH:21]=1)=[O:16])(C)(C)C.NC1C=CC=CC=1NC(C1SC2C=CC(OCCOCCOC)=CC=2C=1)=O>>[NH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[O:18][C:19]2[C:25]([O:26][CH2:27][CH2:28][O:29][CH2:30][CH2:31][O:32][CH3:33])=[CH:24][CH:23]=[CH:22][C:20]=2[CH:21]=1)=[O:16]

Participants

3

Procedure

was prepared from [2-({7-[2-(2-Methoxy-ethoxy)-ethoxy]-benzofuran-2-carbonyl}-amino)-phenyl]-carbamic acid tert-butyl ester (32) in an analogous manner to that described for the preparation of (27) example 11, step 2; exact MW [M+H] calc'd: 371.16; MW found [M+H]: 371.2.

Sources & evidence

ORD record
ord-2d9d25fe53e644ec90b40191b28b21f2
Source dataset
uspto-grants-2007_04
Patent number
US07208491B2

Reaction notes

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