HCID 10362721, compound → HCID 10064886, compound
Reaction equation
C(OC(=O)[NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[NH:18][C:19]2[C:24]([CH:25]=1)=[CH:23][C:22]([O:26][CH2:27][CH2:28][O:29][CH3:30])=[CH:21][CH:20]=2)=[O:16])(C)(C)C.NC1C=CC=CC=1NC(C1SC2C=CC(OCCOCCOC)=CC=2C=1)=O>>[NH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[NH:18][C:19]2[C:24]([CH:25]=1)=[CH:23][C:22]([O:26][CH2:27][CH2:28][O:29][CH3:30])=[CH:21][CH:20]=2)=[O:16]Participants
3
Procedure
was prepared: (2-{[5-(2-Methoxy-ethoxy)-1H-indole-2-carbonyl]-amino}-phenyl)-carbamic acid tert-butyl ester (38) in an analogous manner to that described for the preparation of (27) example 11, step 2; exact MW [M+H] calc'd: 326.15; MW found [M+H]: 326.3.
Workup
- customwas prepared
Sources & evidence
- ORD record
- ord-d73742378ce3454cb2cbc9e36f837dd1
- Source dataset
- uspto-grants-2007_04
- Patent number
- US07208491B2
Reaction notes
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