HCID 10359151, compound → HCID 10064095, compound

HRID 1271864Notes

Reaction equation

HRID 1271864 reaction equation
C(OC(=O)[NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[O:18][C:19]2[C:25]([O:26][CH2:27][CH2:28][O:29][Si](C(C)(C)C)(C)C)=[CH:24][CH:23]=[CH:22][C:20]=2[CH:21]=1)=[O:16])(C)(C)C.NC1C=CC=CC=1NC(C1SC2C=CC(OCCO)=CC=2C=1)=O>>[NH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[NH:14][C:15]([C:17]1[O:18][C:19]2[C:25]([O:26][CH2:27][CH2:28][OH:29])=[CH:24][CH:23]=[CH:22][C:20]=2[CH:21]=1)=[O:16]

Participants

3

Reactant 2

HCID 10359151HCID 10359151, compoundHCID 69490664HCID 69490664, compound

Product 1

HCID 10064095HCID 10064095, compound

Procedure

was prepared from [2-({7-[2-(tert-Butyl-dimethyl-silanyloxy)-ethoxy]-benzofuran-2-carbonyl}-amino)-phenyl]-carbamic acid tert-butyl ester (38) in an analogous manner to that described for the preparation of (39) example 16, step 2; mp. 182–183° C.

Sources & evidence

ORD record
ord-b7a864152a9e45ea977df3b4b7fa796a
Source dataset
uspto-grants-2007_04
Patent number
US07208491B2

Reaction notes

Loading…