HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 2-(4-methoxyphenyl)-N-methylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4-Methoxyphenylacetyl chloride | HCID 2734688 | — |
| Product | 2-(4-methoxyphenyl)-N-methylacetamide | HCID 3264550 | — |
Reaction Steps
was prepared from 4-methoxyphenylacetic acid chloride and methylamine following Method B. 1H NMR (300 MHz, CDCl3) δ 7.14 (d, 2H, J=8.67 Hz), 6.86 (d, 2H, J=8.67 Hz), 3.78 (s, 3H), 3.49 (s, 2H), 2.72 (d, 3H, J=4.71 Hz). LCMS (ESI+) [M+H]/z Calc'd 180, found 180.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07208500B2 |
| Source dataset | uspto-grants-2007_04 |
| ORD ID | ord-d7edd9b82e704228bf097a53b0a08b93 |
| Source note | uspto-grants-2007_04 |