Methyl Isocyanate → HCID 86737553, compound

HRID 127213Notes

Reaction equation

[N:1](=[C:3]1[N:7]=[C:6]([CH2:8][CH3:9])[C:5]([CH3:11])([CH3:10])[S:4]1)[OH:2].[CH3:12][N:13]=[C:14]=[O:15]>>[CH3:12][NH:13][C:14]([O:2][N:1]=[C:3]1[N:7]=[C:6]([CH2:8][CH3:9])[C:5]([CH3:10])([CH3:11])[S:4]1)=[O:15]

Participants

Reactant 2

HCID 12228Methyl Isocyanate

HCID 86737554HCID 86737554, compound

Product 1

HCID 86737553HCID 86737553, compound

Procedure

2-oxo-4-ethyl-5,5-dimethyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4-ethyl-5,5-dimethyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 98°-100° C. The 2-oxo-4-ethyl-5,5-dimethyl-3-thiazoline-oxime starting material (m.p. 178°-180° C.) was prepared from 2-methyl-2-thiocyanato-3-pentanone (b.p. [0.03 mm] 56°-58° C.).

Sources & evidence

ORD record: ord-f84d77e334984c7da09f0c8a38c9fa1c
Source dataset: uspto-grants-1981_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04255436

Reaction notes

Loading…