Methyl Isocyanate → HCID 86737555, compound

Participants

Reaction Steps

2-oxo-4-isopropyl-5,5-dimethyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4-isopropyl-5,5-dimethyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 89°-91° C. The 2-oxo-4-isopropyl-5,5-dimethyl-3-thiazoline-oxime starting material (m.p. 220°-222° C.) was prepared from 2,4-dimethyl-2-thiocyanato-3-pentanone (b.p. [0.02 mm] 64°-66° C.).

Provenance & Evidence