Methyl Isocyanate → HCID 86737563, compound

HRID 127220Notes

Reaction equation

HRID 127220 reaction equation
[N:1](=[C:3]1[N:7]=[C:6]([CH2:8][CH2:9][CH3:10])[C:5]([CH3:12])([CH3:11])[S:4]1)[OH:2].[CH3:13][N:14]=[C:15]=[O:16]>>[CH3:13][NH:14][C:15]([O:2][N:1]=[C:3]1[N:7]=[C:6]([CH2:8][CH2:9][CH3:10])[C:5]([CH3:11])([CH3:12])[S:4]1)=[O:16]

Participants

3

Reactant 2

HCID 12228Methyl IsocyanateHCID 86737564HCID 86737564, compound

Product 1

HCID 86737563HCID 86737563, compound

Procedure

2-oxo-4-propyl-5,5-dimethyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4-propyl-5,5-dimethyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 112°-114° C. The 2-oxo-4-propyl-5,5-dimethyl-3-thiazoline-oxime starting material melts at 145°-147° C.

Sources & evidence

ORD record
ord-4ce41de9107346a2bc8fdfdc13734bc9
Source dataset
uspto-grants-1981_03
Patent number
US04255436

Reaction notes

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