Methyl Isocyanate → HCID 86737565, compound

HRID 127221Notes

Reaction equation

[N:1](=[C:3]1[N:7]=[C:6]([CH:8]2[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]2)[C:5]([CH3:15])([CH3:14])[S:4]1)[OH:2].[CH3:16][N:17]=[C:18]=[O:19]>>[CH3:16][NH:17][C:18]([O:2][N:1]=[C:3]1[N:7]=[C:6]([CH:8]2[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]2)[C:5]([CH3:15])([CH3:14])[S:4]1)=[O:19]

Participants

Reactant 2

HCID 12228Methyl Isocyanate

HCID 86737566HCID 86737566, compound

Product 1

HCID 86737565HCID 86737565, compound

Procedure

2-oxo-4-cyclohexyl-5,5-dimethyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4-cyclohexyl-5,5-dimethyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 158°-160° C. The 2-oxo-4-cyclohexyl-5,5-dimethyl-3-thiazoline-oxime starting material melts at 159°-162° C.

Sources & evidence

ORD record: ord-a726f4d9a6464e7fb8e7335e08581d9f
Source dataset: uspto-grants-1981_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04255436

Reaction notes

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