HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → 2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-O-(methylcarbamoyl)-oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 2-Oxo-4,5-dimethyl-5-ethyl-3-thiazoline-oxime | HCID 85997246 | — |
| Product | 2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-O-(methylcarbamoyl)-oxime | HCID 86737567 | — |
Reaction Steps
2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 115°-117° C. The 2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-oxime starting material melts at 143.5°-144.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04255436 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-90b4a360126f40f9a9ed4a3d8bcb7040 |
| Source note | uspto-grants-1981_03 |