Methyl Isocyanate → HCID 86737568, compound

HRID 127223Notes

Reaction equation

[N:1](=[C:3]1[N:7]=[C:6]([CH2:8][CH3:9])[C:5]([CH2:11][CH3:12])([CH3:10])[S:4]1)[OH:2].[CH3:13][N:14]=[C:15]=[O:16]>>[CH3:13][NH:14][C:15]([O:2][N:1]=[C:3]1[N:7]=[C:6]([CH2:8][CH3:9])[C:5]([CH2:11][CH3:12])([CH3:10])[S:4]1)=[O:16]

Participants

Reactant 2

HCID 12228Methyl Isocyanate

HCID 86737569HCID 86737569, compound

Product 1

HCID 86737568HCID 86737568, compound

Procedure

2-oxo-4,5-diethyl-5-methyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4,5-diethyl-5-methyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 88°-90° C. The 2-oxo-4,5-diethyl-5-methyl-3-thiazoline-oxime starting material melts at 125°-128° C.

Sources & evidence

ORD record: ord-67d30fa3c41b4861a4458b9ba18d1fee
Source dataset: uspto-grants-1981_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04255436

Reaction notes

Loading…