Methyl Isocyanate → HCID 86737570, compound

HRID 127224Notes

Reaction equation

[N:1](=[C:3]1[N:7]=[C:6]([CH3:8])[C:5]([CH3:12])([CH2:9][CH2:10][CH3:11])[S:4]1)[OH:2].[CH3:13][N:14]=[C:15]=[O:16]>>[CH3:13][NH:14][C:15]([O:2][N:1]=[C:3]1[N:7]=[C:6]([CH3:8])[C:5]([CH3:12])([CH2:9][CH2:10][CH3:11])[S:4]1)=[O:16]

Participants

Reactant 2

HCID 12228Methyl Isocyanate

HCID 86737571HCID 86737571, compound

Product 1

HCID 86737570HCID 86737570, compound

Procedure

2-oxo-4,5-dimethyl-5-propyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4,5-dimethyl-5-propyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 66°-69° C. The 2-oxo-4,5-dimethyl-5-propyl-3-thiazoline-oxime starting material melts at 94°-96° C.

Sources & evidence

ORD record: ord-2640e45e980243b0bd6fc28882c11eff
Source dataset: uspto-grants-1981_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04255436

Reaction notes

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