Methyl Isocyanate → HCID 86737572, compound

HRID 127225Notes

Reaction equation

[N:1](=[C:3]1[N:7]=[C:6]([CH2:8][CH2:9][CH3:10])[C:5]([CH2:12][CH3:13])([CH3:11])[S:4]1)[OH:2].[CH3:14][N:15]=[C:16]=[O:17]>>[CH3:14][NH:15][C:16]([O:2][N:1]=[C:3]1[N:7]=[C:6]([CH2:8][CH2:9][CH3:10])[C:5]([CH2:12][CH3:13])([CH3:11])[S:4]1)=[O:17]

Participants

Reactant 2

HCID 12228Methyl Isocyanate

HCID 86737573HCID 86737573, compound

Product 1

HCID 86737572HCID 86737572, compound

Procedure

2-oxo-4-propyl-5-ethyl-5-methyl-3-thiazoline-oxime was reacted with methyl isocyanate as described in Example 4 to yield 2-oxo-4-propyl-5-ethyl-5-methyl-3-thiazoline-O-(methylcarbamoyl)-oxime, m.p. 124°-126° C. The 2-oxo-4-propyl-5-ethyl-5-methyl-3-thiazoline-oxime starting material melts at 132°-135° C.

Sources & evidence

ORD record: ord-3dfbe3a3dd634131ad19ab095e77f85d
Source dataset: uspto-grants-1981_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04255436

Reaction notes

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